39562-22-6
- Product Name：3-Aminocrotonic acid cinnamyl ester
- Molecular Formula：C14H15NO6
- Purity：99%
- Molecular Weight：293.276
Product Details;
CasNo： 39562-22-6
Molecular Formula： C14H15NO6
Appearance： a white crystalline
Manufacturer supply high quality 3-Aminocrotonic acid cinnamyl ester 39562-22-6 with ISO standards
- Molecular Formula:C14H15NO6
- Molecular Weight:293.276
- Appearance/Colour:a white crystalline
- Vapor Pressure:1.03E-07mmHg at 25°C
- Melting Point:72-74 °C
- Refractive Index:1.563
- Boiling Point:433.4 °C at 760 mmHg
- Flash Point:182 °C
- PSA：98.42000
- Density:1.266 g/cm3
- LogP:2.28000
2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate(Cas 39562-22-6) Usage
|
Hazard |
Low toxicity by ingestion and inhalation. A moderate eye irritant. |
InChI:InChI=1/C14H15NO6/c1-10(16)13(14(17)21-7-6-20-2)9-11-4-3-5-12(8-11)15(18)19/h3-5,8-9H,6-7H2,1-2H3
39562-22-6 Relevant articles
Preparation method of cilnidipine
-
Paragraph 0029; 0034; 0038; 0042, (2020/05/08)
The invention discloses a preparation me...
Nimodipine impurity IV reference substance as well as preparation method and application thereof
-
Paragraph 0055-0056, (2020/11/22)
The invention discloses a nimodipine imp...
Design and synthesis of 4-alkyl-2-amino(acetamino)-6-aryl-1,3-thiazine derivatives as influenza neuraminidase inhibitors
Li, Wan,Xia, Lin,Hu, Aixi,Liu, Ailin,Peng, Junmei,Tan, Weiqing
, p. 635 - 644 (2013/09/24)
With a convenient and economical method,...
Dimethylamine benzoate or p-anisate catalysed process for the preparation of 4-(nitrophenyl)-dihydropyridines
-
, (2008/06/13)
PCT No. PCT/EP96/01090 Sec. 371 Date Aug...
39562-22-6 Process route
-
-
22502-03-0
2-methoxyethyl-3-oxobutanoate
-
-
99-61-6
3-nitro-benzaldehyde
-
-
100-09-4
4-methoxybenzoic acid
-
-
39562-22-6
(E/Z)-2-methoxyethyl 2-(3-nitrobenzylidene)-acetoacetate
| Conditions | Yield |
|---|---|
|
With
dimethyl amine;
In
ethanol; isopropyl alcohol;
|
91% |
-
-
22502-03-0
2-methoxyethyl-3-oxobutanoate
-
-
99-61-6
3-nitro-benzaldehyde
-
-
39562-22-6
(E/Z)-2-methoxyethyl 2-(3-nitrobenzylidene)-acetoacetate
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride;
In
toluene;
at 10 ℃;
for 20h;
|
77.5% |
|
With
piperdinium acetate;
In
benzene;
Ambient temperature;
|
73.4% |
|
With
piperidine; acetic acid;
In
benzene;
for 2h;
Heating;
|
|
|
With
piperidine;
In
toluene;
Reflux;
Dean-Stark;
|
|
|
With
sulfuric acid; acetic anhydride;
at 0 - 30 ℃;
Large scale;
|
|
|
With
piperidine; acetic acid;
|
39562-22-6 Upstream products
-
22502-03-0
2-methoxyethyl-3-oxobutanoate
-
99-61-6
3-nitro-benzaldehyde
-
100-09-4
4-methoxybenzoic acid
39562-22-6 Downstream products
-
66085-59-4
nimodipin
-
86387-28-2
(2-methoxy-ethyl) neopentyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate
-
74471-05-9
(2-methoxy-ethyl) trimethylsilyl-methyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate
-
75130-29-9
J-6-163
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